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    高径比气液液搅拌体系的功率响应、油相分布与持气特性

    Power Consumption, Axial Oil Phase Distribution and Gas Holdup in a High-Aspect-Ratio Stirred Vessel with a Gas-Liquid-Liquid System

    • 摘要: 为考察高径比气液液搅拌体系在名义过渡流条件下的功率响应、轴向油相分布及持气特性,以初始体积比为1:1的混合费托α-烯烃/1,2-丙二醇为液液物系,在液位高径比 H/T = 2.10 的三级组合桨搅拌釜内开展冷模实验。实验搅拌转速为130 ~ 300 r·min−1,对应名义搅拌雷诺数 Re 为2827 ~ 6524。结果表明,通气后相对功率消耗和单位体积净输入功率均下降,最大相对功率降幅约为28.4%;提高搅拌转速可减小轴向油相含率差异,而继续增加气体流率对轴向油相分布的影响较小;总体气含率随气体流率和搅拌转速总体升高,但在60 ~ 80 L·min−1范围内增幅较小。综合功率消耗、轴向油相分布和总体气含率结果,40 ~ 60 L·min−1可作为本文装置条件下较适宜的操作气量范围。研究结果可为相近构型气液液搅拌体系的气量选择提供实验参考。

       

      Abstract: Cold model experiments were carried out in a high-aspect-ratio stirred vessel to investigate the effects of aeration on power consumption, axial oil phase distribution and gas holdup in a gas-liquid-liquid system under a nominal transitional flow regime. A mixed Fischer-Tropsch α-olefin/1,2-propanediol liquid-liquid system with an initial volume ratio of 1:1 was used, and air was introduced into a three-stage impeller configuration at a liquid height-to-tank diameter ratio of H/T = 2.10. The stirring speed ranged from 130 to 300 r·min−1, corresponding to a nominal impeller Reynolds number of 2827 to 6524. The results showed that aeration reduced both the relative power consumption and the net power input per unit liquid volume, with a maximum relative power reduction of about 28.4%. When the gas flow rate exceeded 40 L·min−1, the additional power reduction became limited. Increasing the stirring speed reduced the axial difference in local oil phase volume fraction, whereas further increasing the gas flow rate from 40 to 100 L·min−1 did not lead to a continuous change in the axial oil phase distribution. The overall gas holdup generally increased with gas flow rate and stirring speed, but its increment was small when the gas flow rate increased from 60 to 80 L·min−1 under stirred conditions. Considering power consumption, axial oil phase distribution and gas holdup, 40 to 60 L·min−1 was identified as a suitable gas flow rate range under the present experimental conditions.

       

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